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João Paulo de Freitas Grilo completed his Ph.D. in Materials Science and Engineering in 2019, at the University of Aveiro. He graduated in Materials Engineering in 2013, from the Federal University of Rio Grande do Norte (UFRN-Brazil), and he obtained a Postgraduate Certificate in Master of Science in Materials Engineering in 2015, also from the UFRN. Furthermore, he holds a Bachelor's degree in Electrical Technician, which he received in 2009, from the Institute of Federal Education, Science, and Technology of Rio Grande do Norte. Currently, João Paulo de Freitas Grilo is a Researcher at the University of Aveiro. He has an impressive research record, having published 46 articles in various journals and contributed to 4 sections of books. Additionally, he has organized 3 event and participated in 15 others. He has also co-supervised 2 Ph.D. theses and 2 MSc dissertations. João Paulo de Freitas Grilo has been actively involved in multiple research projects, including 3 as a participant, 1 as a Ph.D. Student Fellow, and 1 as a Researcher. He has also contributed to 3 projects as a Scientific Initiation Fellow and served as a Supervisor for 1 project. His research primarily focuses on Engineering and Technology, with a specialization in Materials Engineering, particularly in the field of Ceramics. In his Ciência Vitae curriculum, the most frequently mentioned terms in the context of his scientific and technological output include: Ionic conductor, Solid oxide cells, Mixed conductors, composites, and grain boundary engineering.
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Identification

Personal identification

Full name
João Paulo de Freitas Grilo

Citation names

  • Grilo, João

Author identifiers

Ciência ID
FA11-09FE-10B3
ORCID iD
0000-0001-9917-6142

Email addresses

  • grilo.jpf@ua.pt (Professional)
  • grilo.jpf@gmail.com (Professional)

Telephones

Mobile phone
  • 918802380 (Professional)

Addresses

  • Rua Direita, Bl F1, Cave Direita, 3810001, Aveiro, Aveiro, Portugal (Personal)

Websites

  • https://www.linkedin.com/in/joão-paulo-de-freitas-grilo-5a191479/ (Professional)

Knowledge fields

  • Engineering and Technology - Materials Engineering - Ceramics

Languages

Language Speaking Reading Writing Listening Peer-review
English Advanced (C1) Advanced (C1) Advanced (C1) Advanced (C1) Advanced (C1)
French Intermediate (B1) Intermediate (B1) Elementary (A2) Intermediate (B1) Elementary (A2)
Education
Degree Classification
2022/04/11 - 2022/06/22
Concluded
 Formação Pedagógica Inicial de Formadores (Outros)
SOCIEDADE PROMOTORA DE ESTABELECIMENTOS DE ENSINO, LDA., Portugal
 5 - Excelente
2015/09/01 - 2019/11/11
Concluded
 Materials Science and Engineering (Doutoramento)
Major in Ceramic Materials
Universidade de Aveiro, Portugal
"Ceria-based/carbonates multifunctional composites" (THESIS/DISSERTATION)
 16/20
2013/09/01 - 2015/07/01
Concluded
 Master of Science in Materials Engineering (Postgraduate Certificate)
Major in Ceramic materials for energy conversion system
Universidade Federal do Rio Grande do Norte, Brazil
"NiO-CGO composites obtained by one-step synthesis method" (THESIS/DISSERTATION)
 4.95/5
2008/03/01 - 2013/06/01
Concluded
 Materials Engineering (Graduado)
Major in emphasis on materials applied in the area of oil and natural gas
Universidade Federal do Rio Grande do Norte, Brazil
"YSZ electrolyte evaluation as electrolyte using Co3O4 as sintering aid" (THESIS/DISSERTATION)
 7.9/10
2008/02/01 - 2009/12/01
Concluded
 Electrical Technician (Bachelor)
Major in Medium and high voltage electrical installations
Instituto Federal de Educação Ciência e Tecnologia do Rio Grande do Norte, Brazil
 76/100
Affiliation

Science

Category
Host institution 		Employer
2022/07/01 - Current Researcher (Research) Universidade de Aveiro, Portugal
Universidade de Aveiro CICECO, Portugal
2021/07/01 - 2022/06/30 Researcher (Research) Universidade de Aveiro, Portugal
2019/12/16 - 2021/06/15 Postdoc (Research) Universidade de Aveiro, Portugal
Universidade de Aveiro, Portugal
2017/04/03 - 2017/05/05 Visiting Researcher (Research) Vestel Elektronik, Turkey
Vestel Elektronik, Turkey
2012/08/01 - 2013/07/01 Research Trainee (Research) Universidade Federal do Rio Grande do Norte, Brazil
Universidade Federal do Rio Grande do Norte, Brazil
2010/08/01 - 2012/08/01 Research Trainee (Research) Universidade Federal do Rio Grande do Norte, Brazil
Universidade Federal do Rio Grande do Norte, Brazil
2009/08/01 - 2010/07/01 Research Trainee (Research) Universidade Federal do Rio Grande do Norte, Brazil
Universidade Federal do Rio Grande do Norte, Brazil

Teaching in Higher Education

Category
Host institution 		Employer
2014/10/01 - 2015/07/01 Adjunct Teacher (Polytechnic Teacher) Escola Politécnica do Nordeste, Brazil
Projects

Grant

Designation Funders
2022/07/01 - Current Innovative solutions for grain boundary engineering in ionic and mixed ceramic conductors
2021.04328.CEECIND
Supervisor
Universidade de Aveiro CICECO, Portugal
 Associação para a Inovação e Desenvolvimento da FCT
Ongoing
2019/12/16 - 2022/06/30 MERIT – Microstructural Engineering Route for Enhanced Interfacial Ionic Transport
POCI-01-0145-FEDER-028612
Researcher
Fundação para a Ciência e a Tecnologia
2012/08/01 - 2013/07/01 Study of the wetting of mechanically metallized ceramics for metal/ceramic brazing
PIBIC/CNPq Ref. PVG7055-2012
Scientific Initiation Fellow
Universidade Federal do Rio Grande do Norte, Brazil
 Coordenação de Aperfeiçoamento de Pessoal de Nível Superior
Concluded
2010/08/01 - 2012/08/01 Processing and analysis of materials used in the oil and gas industry
PRH-ANP/MT30
Scientific Initiation Fellow
Agência Nacional do Petróleo Gás Natural e Biocombustíveis
Concluded
2010/08 - 2012/08 Processing and analysis of materials used in the oil and gas industry
PRH-ANP/MT30
 Agência Nacional do Petróleo Gás Natural e Biocombustíveis

Contract

Designation Funders
2017/09/01 - 2020/08/31 novel molten carbonate/ceramic composite materials for sustainable energy technologies with. co2 capture and utilization
FCT ref. M-ERA-NET2/0009/2016
Member
Universidade de Aveiro, Portugal
 Fundação para a Ciência e a Tecnologia
Concluded
2015/09/01 - 2019/08/01 Multifunctional composite electrolytes based on ceria and molten carbonates
205102/2014-0.
PhD Student Fellow
Universidade de Aveiro, Portugal

Universidade de Aveiro CICECO, Portugal
Conselho Nacional de Desenvolvimento Científico e Tecnológico
Concluded
2016/01/01 - 2019/01/01 zero co2 emissions: challenge and foresight for innovative multi-ionic functional membranes
FCT Ref PTDC/CTM-CER/6732/2014
Member
Fundação para a Ciência e a Tecnologia
Concluded
2014/01/01 - 2018/01/01 Nano-composites based on ceria and molten salts for hybrid fuel cells of intermediate temperatures (400 to 600ºC) with electrolytes
MEC/MCTI/CAPES/CNPq/FAPs nº 03/2014
Mebro
Coordenação de Aperfeiçoamento de Pessoal de Nível Superior
Concluded
2014/07/01 - 2017/09/30 Nanomateriais compósitos multifuncionais para pilhas de combustível de baixa temperatura
New-INDIGO/0001/2013
Universidade de Aveiro, Portugal

Universidade de Aveiro CICECO, Portugal
Fundação para a Ciência e a Tecnologia
Concluded

Other

Designation Funders
2009/08/01 - 2010/08/01 New materials for nuclear power plants
PIBIC/CNPq Ref. PVG2629-2009
Scientific Initiation Fellow
Concluded
Outputs

Publications

Book chapter
  1. Loureiro, F.J.A.; Silva, V.D.; Simões, T.A.; Cesário, M.R.; Grilo, J.P.F.; Fagg, D.P.; Macedo, D.A.. "Misfit-layered Ca-cobaltite-based cathodes for intermediate-temperature solid oxide fuel cell". 347-377. 2019.
  2. Santos, Gabriel M.; de F. Grilo, Joao P.; do Nascimento, Rubens M.; Paskocimas, Carlos A.; Cesario, Moisés R.; de Macedo, Daniel A.; de Araujo, Allan J.M.. "NiO-Ce0.9Gd0.1O1.95 Composites and their Cermets as Anode Materials for SOFC". In Catalytic Materials for Hydrogen Production and Electro-oxidation Reactions, 162-197. BENTHAM SCIENCE PUBLISHERS, 2018.
    10.2174/9781681087580118020009
  3. Paulo de Freitas Grilo, João; Gomes Moura, Caroline; Araújo de Macedo, Daniel. "Introduction to Solid Oxide Fuel Cells". In Frontiers in Ceramic Science, 3-8. BENTHAM SCIENCE PUBLISHERS, 2017.
    10.2174/9781681084312117010005
  4. Gomes Moura, Caroline; Paulo de Freitas Grilo, João; Maribondo do Nascimento, Rubens; Araújo de Macedo, Daniel. "A Brief Review on Anode Materials and Reactions Mechanism in Solid Oxide Fuel Cells". In Frontiers in Ceramic Science, 26-41. BENTHAM SCIENCE PUBLISHERS, 2017.
    10.2174/9781681084312117010007
Conference paper
  1. Grilo, João; R. M. Nascimento. "Effect of Co3O4 addition on densification of 8 mol% yttria stabilized zirconia". Paper presented in 56th Brazilian congress on ceramics; 1st Latin American congress on ceramics; 9th BraSyGlass: Brazilian symposium on glass and related materials;, Curitiba, 2012.
    Published
  2. Grilo, João; P. P. B. Neto,; R. M. Nascimento. "Co-sintering of CGO/NIO-CGO bilayers for solid oxide fuel cell". Paper presented in 56th Brazilian congress on ceramics; 1st Latin American congress on ceramics; 9th BraSyGlass: Brazilian symposium on glass and related materials;, Curitiba, 2012.
    Published
  3. Grilo, João; R. M. Nascimento. "Effect of Co3O4 content on sintering and microstructure of 4 mol% yttria stabilized zirconia ceramics". Paper presented in 55th Brazilian congress on ceramics, 2011.
    Published
Conference poster
  1. Gabija Navašinskaite; Grilo, João; Francielly Roussenq Cesconeto. Corresponding author: Gabija Navašinskaite. "Exploring the Use of Recycled Glass and Alkali Salts in Alumina-Based Composites for LTCC Technology". Paper presented in Jornadas CICECO 2023, 2023.
  2. Grilo, João; Miguel Illesca; Cesconeto, F.R.. "Assessment of electrical properties of cellular ceria-based composites". Paper presented in 20th International Conference on Advanced Nanomaterials-ANM - AEM - Alternative Energy Materials, 2023.
  3. Grilo, João; F. M. B. Marques. "Electrical properties of composites: impact of distinct processing routes". Paper presented in Electroceramics XVII, 2020.
  4. J. P. F. Grilo; F. M. B. Marques. "On the electronic conductivity of Gd-doped ceria with added salts". Paper presented in 14th Spanish National Meeting on Electroceramics, 2019.
  5. Grilo, João. "Electrochemical assessment of NiO-CGO nanocomposites as cermet precursors". Paper presented in 43rd International Conference and Exposition on Advanced Ceramics and Composites (ICACC 2019), 2019.
  6. Grilo, João. "NiO-CGO nanocomposites as cermet precursors". Paper presented in 5th International Conference on Nanotechnology, Nanomaterials & Thin Films for Energy Applications, 2018.
  7. Grilo, João; F. M. B. Marques. "(Na,Li)2CO3 interaction with Gd-doped ceria in composite electrolytes". Paper presented in Electroceramics XVI, 2018.
  8. Grilo, João; Fernando Manoel Bico Marques. "Sintering of nano Ce0.9Gd0.1O1.95 powders with alkali carbonates". Paper presented in 9th International Conference on Advanced Nanomaterials-ANM, 2017.
  9. Grilo, João; Fernando Manoel Bico Marques. "Alkaline Carbonates as Sintering Aid for Ce0.9Gd0.1O1.95". Paper presented in 15th Conference & Exhibition of the European Ceramic Society, 2017.
  10. Grilo, João. "NiO-GDC composites obtained by one-step synthesis". Paper presented in 7th International Conference on Advanced Nanomaterials-ANM, 2016.
  11. Grilo, João; Rubens Maribondo do Nascimento. "sintering and microstructure of NiO/Ni-YSZ anode materials". Paper presented in XIII Brazilian Materials Research Society Meeting, 2014.
  12. Grilo, João; Rubens Maribondo do Nascimento. "Preparação de meia-células LSCF/YSZ-Co3O4 por brush painting". Paper presented in 57º Congresso Brasileiro de Cerâmica, 2013.
  13. Grilo, João; Paulo Neto; Rubens Maribondo do Nascimento. "Efeito da adição do Co3O4 na densificação da zircônia estabilizada com 8% mol de ítria". Paper presented in 56º Congresso Brasileiro de Cerâmica, 2012.
  14. Grilo, João; Rubens Maribondo do Nascimento. "Efeito do teor de Co3O4 na sinterização e microestrutura de cerâmicas de zircônia 4% mol de ítria". Paper presented in 55º Congresso Brasileiro de Cerâmica, Porto de Galinhas, 2011.
Journal article
  1. Starykevich, M.; Rondão, A.I.B.; Grilo, J.P.F.; Marques, F.M.B.. "Tuning of phase content, microstructure and thermal expansion of MgPSZ". Ceramics International 49 3 (2023): 5401-5408. http://www.scopus.com/inward/record.url?eid=2-s2.0-85144244280&partnerID=MN8TOARS.
    10.1016/j.ceramint.2022.10.063
  2. Araújo, Allan J.M.; Loureiro, Francisco J.A.; Grilo, João P.F.; Macedo, Daniel A.; Paskocimas, Carlos A.; Fagg, Duncan P.. "A high-performance oxygen electrode for solid oxide cells: Compositional optimisation of barium cobaltite-based composites". Journal of Alloys and Compounds 906 (2022): 164382. http://dx.doi.org/10.1016/j.jallcom.2022.164382.
    10.1016/j.jallcom.2022.164382
  3. Rondão, A.I.B.; Grilo, J.P.F.; Starykevich, M.; Marques, F.M.B.. "Dilatometric inspection of phase changes in Mg-PSZ". Thermochimica Acta 709 (2022): 179147. http://dx.doi.org/10.1016/j.tca.2022.179147.
    10.1016/j.tca.2022.179147
  4. Araújo, A.J.M.; Loureiro, F.J.A.; Grilo, J.P.F.; Macedo, D.A.; Paskocimas, C.A.; Fagg, D.P.. "Changing the oxygen reaction mechanism in composite electrodes by the addition of ionic- or ambipolar-conducting phases: Series or parallel pathways". Electrochimica Acta 418 (2022): http://www.scopus.com/inward/record.url?eid=2-s2.0-85128714493&partnerID=MN8TOARS.
    10.1016/j.electacta.2022.140383
  5. Rondão, A.I.B.; Grilo, J.P.F.; Starykevich, M.; Dias, D.M.C.; Marques, F.M.B.. "High temperature ionic and electronic conductivity in MgPSZ". Solid State Ionics 385 (2022): http://www.scopus.com/inward/record.url?eid=2-s2.0-85137812988&partnerID=MN8TOARS.
    10.1016/j.ssi.2022.116009
  6. Starykevich, M.; Rondão, A.I.B.; Grilo, J.P.F.; Marques, F.M.B.. "Role of the monoclinic phase on the thermal and electrical performance of MgPSZ". MRS Communications 12 5 (2022): 831-837. http://www.scopus.com/inward/record.url?eid=2-s2.0-85137578049&partnerID=MN8TOARS.
    10.1557/s43579-022-00249-7
  7. Araújo, A.J.M.; Loureiro, F.J.A.; Holz, L.I.V.; Graça, V.C.D.; Grilo, J.P.F.; Macedo, D.A.; Paskocimas, C.A.; Fagg, D.P.. "Boosted electrochemical performance of ca-cobaltite-based composite electrodes for reversible solid oxide cells". International Journal of Energy Research 46 15 (2022): 22070-22077. http://www.scopus.com/inward/record.url?eid=2-s2.0-85130741497&partnerID=MN8TOARS.
    10.1002/er.8174
  8. Grilo, J.P.F.; Jamale, A.; Starykevich, M.; Figueiredo, F.M.L.; Marques, F.M.B.. "Role of salts on the electrical performance of ceria-based electrolytes: An overview". Frontiers in Materials 9 (2022): http://www.scopus.com/inward/record.url?eid=2-s2.0-85139760623&partnerID=MN8TOARS.
    10.3389/fmats.2022.993583
  9. Cesario, Moisés R.; Souza, Glageane S.; Loureiro, Francisco J.A.; Araújo, Allan J.M.; Grilo, João P.F.; Aouad, Samer; Tidahy, Haingomalala L.; et al. "Synthesis of Co–Ni and Cu–Ni based-catalysts for dry reforming of methane as potential components for SOFC anodes". Ceramics International 47 23 (2021): 33191-33201. http://dx.doi.org/10.1016/j.ceramint.2021.08.220.
    10.1016/j.ceramint.2021.08.220
  10. Araújo, Pedro A.S.; Andrade, Rivaildo M.; Araújo, Allan J.M.; Raimundo, Rafael A.; Grilo, João P.F.; Dutra, Ricardo P.S.; Macedo, Daniel A.; Nascimento, Rubens M.. "Cordierite-based ceramics with coffee husk ash addition: I –microstructure and physical properties". Journal of Materials Research and Technology 15 (2021): 2471-2483. http://dx.doi.org/10.1016/j.jmrt.2021.09.032.
    10.1016/j.jmrt.2021.09.032
  11. Araújo, Allan J.M.; Loureiro, Francisco J.A.; Holz, Laura I.V.; Graça, Vanessa C.D.; Grilo, João P.F.; Macedo, Daniel A.; Paskocimas, Carlos A.; Fagg, Duncan P.. "Creating new surface-exchange pathways on the misfit Ca-cobaltite electrode by the addition of an active interlayer". Journal of Power Sources 510 (2021): 230417. http://dx.doi.org/10.1016/j.jpowsour.2021.230417.
    10.1016/j.jpowsour.2021.230417
  12. Araújo, Allan J.M.; Loureiro, Francisco J.A.; Holz, Laura I.V.; Grilo, João P.F.; Macedo, Daniel A.; Paskocimas, Carlos A.; Fagg, Duncan P.. "Composite of calcium cobaltite with praseodymium-doped ceria: A promising new oxygen electrode for solid oxide cells". International Journal of Hydrogen Energy 46 55 (2021): 28258-28269. http://dx.doi.org/10.1016/j.ijhydene.2021.06.049.
    10.1016/j.ijhydene.2021.06.049
  13. Lima, Chrystian G.M.; Araújo, Allan J.M.; Silva, Rinaldo M.; Raimundo, Rafael A.; Grilo, João P.F.; Constantinescu, Gabriel; Kovalevsky, Andrei V.; Macedo, Daniel A.. "Electrical assessment of brownmillerite-type calcium ferrite materials obtained by proteic sol-gel route and by solid-state reaction using mollusk shells". Journal of Solid State Chemistry 299 (2021): 122172. http://dx.doi.org/10.1016/j.jssc.2021.122172.
    10.1016/j.jssc.2021.122172
  14. Garcia, Maxwell F.L.; Araújo, Allan J.M.; Raimundo, Rafael A.; Nascimento, Rubens M.; Grilo, João P.F.; Macedo, Daniel A.. "Electrical properties of Ca-doped ceria electrolytes prepared by proteic sol-gel route and by solid-state reaction using mollusk shells". International Journal of Hydrogen Energy 46 33 (2021): 17374-17387. http://dx.doi.org/10.1016/j.ijhydene.2021.02.151.
    10.1016/j.ijhydene.2021.02.151
  15. Silva, Vinícius D.; Nascimento, Emanuel P.; Grilo, João P.F.; Simões, Thiago A.; Menezes, Romualdo R.; Macedo, Daniel A.; Medeiros, Eliton S.. "Effect of two-step calcination on the formation of nickel oxide hollow nanofibers". Open Ceramics 5 (2021): 100087. http://dx.doi.org/10.1016/j.oceram.2021.100087.
    10.1016/j.oceram.2021.100087
  16. Grilo, J.P.F.; Macedo, D.A.; Nascimento, R.M.; Marques, F.M.B.. "Assessment of processing route on the performance of ceria-based composites". International Journal of Energy Research (2021): http://www.scopus.com/inward/record.url?eid=2-s2.0-85100298988&partnerID=MN8TOARS.
    10.1002/er.6438
  17. Grilo, J.P.F.; Macedo, D.A.; Nascimento, R.M.; Marques, F.M.B.. "Innovative improvement of sintered ceramic electrolytes by salt infiltration". Ceramics International 47 4 (2021): 5079-5090. http://www.scopus.com/inward/record.url?eid=2-s2.0-85094864718&partnerID=MN8TOARS.
    10.1016/j.ceramint.2020.10.086
  18. Grilo, João. "Performance of GDC with alkali metal carbonates as sintering aids". Solid State Ionics (2020): http://dx.doi.org/10.1016/j.ssi.2020.115221.
    10.1016/j.ssi.2020.115221
  19. Silva, V.D.; Simões, T.A.; Grilo, J.P.F.; Medeiros, E.S.; Macedo, D.A.. "Impact of the NiO nanostructure morphology on the oxygen evolution reaction catalysis". Journal of Materials Science 55 15 (2020): 6648-6659. http://www.scopus.com/inward/record.url?eid=2-s2.0-85079672433&partnerID=MN8TOARS.
    10.1007/s10853-020-04481-1
  20. Araújo, A.J.M.; Grilo, J.P.F.; Loureiro, F.J.A.; Holz, L.I.V.; Macedo, D.A.; Fagg, D.P.; Paskocimas, C.A.. "Proteic sol–gel synthesis of Gd-doped ceria: a comprehensive structural, chemical, microstructural and electrical analysis". Journal of Materials Science 55 36 (2020): 16864-16878. http://www.scopus.com/inward/record.url?eid=2-s2.0-85091207629&partnerID=MN8TOARS.
    10.1007/s10853-020-05173-6
  21. Carregosa, J.D.C.; Grilo, J.P.F.; Godoi, G.S.; Macedo, D.A.; Nascimento, R.M.; Oliveira, R.M.P.B.. "Microwave-assisted hydrothermal synthesis of ceria (CeO2): Microstructure, sinterability and electrical properties". Ceramics International 46 14 (2020): 23271-23275. http://www.scopus.com/inward/record.url?eid=2-s2.0-85086514061&partnerID=MN8TOARS.
    10.1016/j.ceramint.2020.06.021
  22. Silva, V.D.; Ferreira, L.S.; Araújo, A.J.M.; Simões, T.A.; Grilo, J.P.F.; Tahir, M.; Medeiros, E.S.; Macedo, D.A.. "Ni and Ce oxide-based hollow fibers as battery-like electrodes". Journal of Alloys and Compounds 830 (2020): http://www.scopus.com/inward/record.url?eid=2-s2.0-85081029247&partnerID=MN8TOARS.
    10.1016/j.jallcom.2020.154633
  23. Araújo, A.J.M.; Silva, V.D.; Sousa, A.R.O.; Grilo, J.P.F.; Simões, T.A.; Macedo, D.A.; Nascimento, R.M.; Paskocimas, C.A.. "Battery-like behavior of Ni-ceria based systems: Synthesis, surface defects and electrochemical assessment". Ceramics International 45 6 (2019): 7157-7165. http://www.scopus.com/inward/record.url?eid=2-s2.0-85059344587&partnerID=MN8TOARS.
    10.1016/j.ceramint.2018.12.222
  24. Loureiro, F.J.A.; Macedo, D.A.; Nascimento, R.M.; Cesário, M.R.; Grilo, J.P.F.; Yaremchenko, A.A.; Fagg, D.P.. "Cathodic polarisation of composite LSCF-SDC IT-SOFC electrode synthesised by one-step microwave self-assisted combustion". Journal of the European Ceramic Society 39 5 (2019): 1846-1853. http://www.scopus.com/inward/record.url?eid=2-s2.0-85059695201&partnerID=MN8TOARS.
    10.1016/j.jeurceramsoc.2019.01.013
  25. Grilo, J.P.F.; Alves, H.P.A.; Araújo, A.J.M.; Andrade, R.M.; Dutra, R.P.S.; Macedo, D.A.. "Dielectric and electrical properties of a mullite/glass composite from a kaolinite clay/mica-rich kaolin waste mixture,(Propriedades dielétricas e elétricas de compósito mulita/fase vítrea obtido a partir de uma mistura argila caulinítica/resíduo de caulim)". Ceramica 65 373 (2019): 117-121. http://www.scopus.com/inward/record.url?eid=2-s2.0-85061113673&partnerID=MN8TOARS.
    10.1590/0366-69132019653732648
  26. Grilo, J.P.F.; Macedo, D.A.; Nascimento, R.M.; Marques, F.M.B.. "Electronic conductivity in Gd-doped ceria with salt additions". Electrochimica Acta 318 (2019): 977-988. http://www.scopus.com/inward/record.url?eid=2-s2.0-85068140267&partnerID=MN8TOARS.
    10.1016/j.electacta.2019.06.148
  27. Andrade, R.M.; Araújo, A.J.; Alves, H.P.; Grilo, J.P.; Dutra, R.P.; Campos, L.F.; Macedo, D.A.. "On the physico-mechanical, electrical and dielectric properties of mullite-glass composites". Ceramics International (2019): http://www.scopus.com/inward/record.url?eid=2-s2.0-85068007837&partnerID=MN8TOARS.
    10.1016/j.ceramint.2019.06.070
  28. Emerenciano, A.A.; Araújo, A.J.M.; Grilo, J.P.F.; Macedo, D.A.; Rasekh, S.; Kovalevsky, A.V.; Paskocimas, C.A.; Nascimento, R.M.. "Environmentally friendly synthesis methods to obtain the misfit [Ca2CoO3-d]0.62[CoO2] thermoelectric material". Materials Letters 254 (2019): 286-289. http://www.scopus.com/inward/record.url?eid=2-s2.0-85069872604&partnerID=MN8TOARS.
    10.1016/j.matlet.2019.07.053
  29. Loureiro, F.J.A.; Souza, G.S.; Graça, V.C.D.; Araújo, A.J.M.; Grilo, J.P.F.; Macedo, D.A.; Fagg, D.P.. "Nickel-copper based anodes for solid oxide fuel cells running on hydrogen and biogas: Study using ceria-based electrolytes with electronic short-circuiting correction". Journal of Power Sources 438 (2019): http://www.scopus.com/inward/record.url?eid=2-s2.0-85070916568&partnerID=MN8TOARS.
    10.1016/j.jpowsour.2019.227041
  30. Santos, T.H.; Grilo, J.P.F.; Loureiro, F.J.A.; Fagg, D.P.; Fonseca, F.C.; Macedo, D.A.. "Structure, densification and electrical properties of Gd3+ and Cu2+ co-doped ceria solid electrolytes for SOFC applications: Effects of Gd2O3 content". Ceramics International 44 3 (2018): 2745-2751. http://www.scopus.com/inward/record.url?eid=2-s2.0-85034418453&partnerID=MN8TOARS.
    10.1016/j.ceramint.2017.11.009
  31. Santos, J.R.D.; Loureiro, F.J.A.; Grilo, J.P.F.; Silva, V.D.; Simões, T.A.; Fagg, D.P.; Macedo, D.A.. "Understanding the cathodic polarisation behaviour of the misfit [Ca2CoO3-d]q[CoO2] (C349) as oxygen electrode for IT-SOFC". Electrochimica Acta 285 (2018): 214-220. http://www.scopus.com/inward/record.url?eid=2-s2.0-85051117241&partnerID=MN8TOARS.
    10.1016/j.electacta.2018.08.018
  32. Grilo, J.P.F.; Macedo, D.A.; Nascimento, R.M.; Marques, F.M.B.. "Assessment of NiO-CGO composites as cermet precursors". Solid State Ionics 321 (2018): 115-121. http://www.scopus.com/inward/record.url?eid=2-s2.0-85046035714&partnerID=MN8TOARS.
    10.1016/j.ssi.2018.04.014
  33. Silva, V.D.; Silva, R.M.; Grilo, J.P.F.; Loureiro, F.J.A.; Fagg, D.P.; Medeiros, E.S.; Macedo, D.A.. "Electrochemical assessment of novel misfit Ca-cobaltite-based composite SOFC cathodes synthesized by solution blow spinning". Journal of the European Ceramic Society 38 6 (2018): 2562-2569. http://www.scopus.com/inward/record.url?eid=2-s2.0-85041617102&partnerID=MN8TOARS.
    10.1016/j.jeurceramsoc.2018.01.044
  34. Silva, R.M.; Raimundo, R.A.; Fernandes, W.V.; Torres, S.M.; Silva, V.D.; Grilo, J.P.F.; Morales, M.A.; Macedo, D.A.. "Proteic sol-gel synthesis, structure and magnetic properties of Ni/NiO core-shell powders". Ceramics International 44 6 (2018): 6152-6156. http://www.scopus.com/inward/record.url?eid=2-s2.0-85039913292&partnerID=MN8TOARS.
    10.1016/j.ceramint.2017.12.248
  35. Araújo, A.J.M.; Grilo, J.P.F.; Loureiro, F.J.A.; Campos, L.F.A.; Paskocimas, C.A.; Nascimento, R.M.; Macedo, D.A.. "Designing experiments for the preparation of Ni-GDC cermets with controlled porosity as SOFC anode materials: effects on the electrical properties". Ceramics International 44 18 (2018): 23088-23093. http://www.scopus.com/inward/record.url?eid=2-s2.0-85053328591&partnerID=MN8TOARS.
    10.1016/j.ceramint.2018.09.115
  36. Sousa, Angel R.O.; Araujo, Allan J.M.; Souza, Glageane S.; Grilo, João P.F.; Loureiro, Francisco J.A.; Fagg, Duncan P.; Macedo, Daniel A.. "Electrochemical assessment of one-step Cu-CGO cermets under hydrogen and biogas fuels". Materials Letters 191 (2017): 141-144. http://dx.doi.org/10.1016/j.matlet.2016.12.087.
    10.1016/j.matlet.2016.12.087
  37. Moura, C.G.; Pereira, R.S.F.; Andritschky, M.; Lopes, A.L.B.; Grilo, J.P.D.F.; Nascimento, R.M.D.; Silva, F.S.. "Effects of laser fluence and liquid media on preparation of small Ag nanoparticles by laser ablation in liquid". Optics and Laser Technology 97 (2017): 20-28. http://www.scopus.com/inward/record.url?eid=2-s2.0-85021152433&partnerID=MN8TOARS.
    10.1016/j.optlastec.2017.06.007
  38. Fulgêncio, E.B.G.A.; Melo, K.P.V.; Silva, R.M.; Grilo, J.P.F.; Caignaert, V.; Cesário, M.R.; Campos, L.F.A.; Macedo, D.A.. "Misfit Ca-cobaltite from a mixture of mollusk shells and cobalt oxide as potential SOFC cathode material". Ceramics International 43 12 (2017): 9564-9567. http://www.scopus.com/inward/record.url?eid=2-s2.0-85018906370&partnerID=MN8TOARS.
    10.1016/j.ceramint.2017.04.099
  39. Grilo, J.P.F.; Moura, C.G.; Macedo, D.A.; Rajesh, S.; Figueiredo, F.M.L.; Marques, F.M.B.; Nascimento, R.M.. "Effect of composition on the structural development and electrical conductivity of NiO-GDC composites obtained by one-step synthesis". Ceramics International 43 12 (2017): 8905-8911. http://www.scopus.com/inward/record.url?eid=2-s2.0-85017233966&partnerID=MN8TOARS.
    10.1016/j.ceramint.2017.04.027
  40. Sousa, A.R.O.; Araujo, A.J.M.; Souza, G.S.; Grilo, J.P.F.; Loureiro, F.J.A.; Fagg, D.P.; Macedo, D.A.. "Electrochemical assessment of one-step Cu-CGO cermets under hydrogen and biogas fuels". Materials Letters 191 (2017): 141-144. http://www.scopus.com/inward/record.url?eid=2-s2.0-85008474317&partnerID=MN8TOARS.
    10.1016/j.matlet.2016.12.087
  41. Alves, H.P.A.; Junior, R.A.; Campos, L.F.A.; Dutra, R.P.S.; Grilo, J.P.F.; Loureiro, F.J.A.; Macedo, D.A.. "Structural study of mullite based ceramics derived from a mica-rich kaolin waste". Ceramics International 43 4 (2017): 3919-3922. http://www.scopus.com/inward/record.url?eid=2-s2.0-85007049096&partnerID=MN8TOARS.
    10.1016/j.ceramint.2016.12.035
  42. Silva, T.H.S.; Lima, C.G.M.; Dutra, R.P.S.; De M Aquino, F.; Grilo, J.P.F.; Rajesh, S.; Macedo, D.A.. "Effects of gadolinia doping on densification and electrical properties of Ce0.99-xGdxCu0.01O2-d solid solutions,Efeitos da dopagem com gadolínia na densificação e nas propriedades elétricas de soluções sólidas Ce0,99-xGdxCu0,01O2-d". Ceramica 63 368 (2017): 470-477. http://www.scopus.com/inward/record.url?eid=2-s2.0-85037843672&partnerID=MN8TOARS.
    10.1590/0366-69132017633682141
  43. Medeiros, S.G.; Dutra, R.P.S.; Grilo, J.P.F.; Martinelli, A.E.; Paskocimas, C.A.; Macedo, D.A.. "Preparation of low-cost alumina-mullite composites via reactive sintering between a kaolinite clay from Paraíba and aluminum hydroxide,Preparação de compósitos alumina-mulita de baixo custo via sinterização reativa entre uma argila caulinítica da Paraíba e hidróxido de alumínio". Ceramica 62 363 (2016): 266-271. http://www.scopus.com/inward/record.url?eid=2-s2.0-84990924658&partnerID=MN8TOARS.
    10.1590/0366-69132016623631992
  44. Moura, C.G.; Grilo, J.P.D.F.; Macedo, D.A.; Cesário, M.R.; Fagg, D.P.; Nascimento, R.M.. "Cobalt-free perovskite Pr0.5Sr0.5Fe1-xCuxO3-d (PSFC) as a cathode material for intermediate temperature solid oxide fuel cells". Materials Chemistry and Physics 180 (2016): 256-262. http://www.scopus.com/inward/record.url?eid=2-s2.0-84991000998&partnerID=MN8TOARS.
    10.1016/j.matchemphys.2016.06.005
  45. Araujo, A.J.M.; Sousa, A.R.O.; Grilo, J.P.F.; Campos, L.F.A.; Loureiro, F.J.A.; Fagg, D.P.; Dutra, R.P.S.; Macedo, D.A.. "Preparation of one-step NiO/Ni-CGO composites using factorial design". Ceramics International 42 16 (2016): 18166-18172. http://www.scopus.com/inward/record.url?eid=2-s2.0-84994112962&partnerID=MN8TOARS.
    10.1016/j.ceramint.2016.08.131
  46. Lima, C.G.M.; Santos, T.H.; Grilo, J.P.F.; Dutra, R.P.S.; Nascimento, R.M.; Rajesh, S.; Fonseca, F.C.; Macedo, D.A.. "Synthesis and properties of CuO-doped Ce0.9Gd0.1O2-d electrolytes for SOFCs". Ceramics International 41 3 (2015): 4161-4168. http://www.scopus.com/inward/record.url?eid=2-s2.0-84921824213&partnerID=MN8TOARS.
    10.1016/j.ceramint.2014.12.093
Activities

Oral presentation

Presentation title Event name
Host (Event location)
2022/07/29 Assessment of processing route on the electrical properties of Ce0.9Gd0.1O1.95 and (Na, Li)2CO3 composites International Conference on Advanced Nanomaterials-ANM
Universidade de Aveiro (Aveiro, Portugal)
2020/08/24 Grain boundary conductivity enhancement by salt infiltration Electroceramics XVII
(Darmstadt, Germany)
2019/07/13 Electrical assessment of Ce0.9Gd0.1O1.95 with added alkaline salts 16th Conference & Exhibition of the European Ceramic Society
(Torino, Italy)
2018/07/09 Sintering admixtures for tuned porosity CGO matrices Electroceramics XVI
(Hasselt, Belgium)

Supervision

Thesis Title
Role 		Degree Subject (Type)
Institution / Organization
2024/02/01 - Current IMPACTO DA ADIÇÃO DE CsVO3 /MoO 3 EM SAIS FUNDIDOS DE MEMBRANAS COMPÓSITAS PARA SEPARAÇÃO DE CO2
Supervisor
 Ciência e Engenharia de Materiais (Master)
Universidade de Aveiro, Portugal
2023/06/01 - Current Estudo do uso da casca beneficiada do ovo na substituição de matéria prima comercial na produção de Varistor de ZnO usando a síntese de reação de combustão
Co-supervisor
 Graduate Program in Materials Science and Engineering (PhD)
Universidade Federal da Paraíba, Brazil
2019/12/16 - 2021/12/16 Eletrodos à base de cobaltita de cálcio para aplicações energética (Calcium cobaltite electrodes for energy applications).
Co-supervisor of Klivia Pricillia De Vasconcelos Mélo
 Materials Science and Engineering (Master)
Universidade Federal da Paraíba, Brazil
2020/04/01 - 2021/04/03 Processamento, microestrutura e propriedades elétricas de céria cálcia (Processing, microstructure and electrical properties of ceria-calcium).
Co-supervisor of Maxwell Ferreira de Lima Garcia
 Materials Science and Engineering (PhD)
Universidade Federal da Paraíba, Brazil

Event organisation

Event name
Type of event (Role) 		Institution / Organization
2023/07/26 - 2023/07/28 Organising committee of Advanced Nano Materials conference (2023/07/26 - 2023/07/28)
Conference (Member of the Organising Committee)
 Universidade de Aveiro, Portugal
2022/07/27 - 2022/07/29 Organising committee of Advanced Nano Materials conference (2022/07/27 - 2022/07/29)
Conference (Member of the Organising Committee)
 Universidade de Aveiro, Portugal
2017/07/19 - 2017/07/21 Organising committee of Advanced Nano Materials conference (2017/07/19 - 2017/07/21)
Conference (Member of the Organising Committee)
 Universidade de Aveiro, Portugal

Event participation

Activity description
Type of event 		Event name
Institution / Organization
2020/06/19 - 2020/08/21 Ceramic with high ionic mobility: applications and challenges, 15 h course.
Other
Universidade Federal da Paraíba, Brazil
2019/06/11 - 2019/06/12 Jornadas CICECO 2019, Where Science meets Societ.
Meeting
 Jornadas CICECO 2019
Universidade de Aveiro CICECO, Portugal
2019/01/25 - 2019/01/29 ACerS Winter workshop.
Workshop
 ACerS Winter Workshop
2018/08/20 - 2018/08/24 3rd International Summer School Kaunas University of Technology, Palanga, Lithuania, 20th – 24th August 2018.
Other
 3rd International Summer School Kaunas University of Technology
Kauno Technologijos Universitetas Socialiniu Mokslu Fakultetas, Lithuania
2018/07/18 - 2018/07/20 Poster presentation. NiO-CGO nanocomposites as cermet precursors. Aveiro, Portugal, July 18 – 20, 2018.
Conference
 5th International Conference on Nanotechnology, Nanomaterials & Thin Films for Energy Applications
2018/07/09 - 2018/07/12 Poster presentation. (Na,Li)2CO3 interaction with Gd-doped ceria in composite electrolytes. Hasselt, Belgium.
Conference
 Electroceramics XVI
2017/09/12 - 2017/09/12 Workshop: Good Practices in Education in Science and Technology of Materials and Ceramic Materials
Workshop
 Workshop: Good Practices in Education in Science and Technology of Materials and Ceramic Materials, EUCERMAT
Universidade de Aveiro, Portugal
2017/07/19 - 2017/07/21 Poster presentation. Sintering of nano Ce0.9Gd0.1O1.95 powders with alkali carbonates. Aveiro, Portugal.
Conference
 9th International Conference on Advanced Nanomaterials-ANM
2017/07/09 - 2017/07/13 Poster presentation. Alkaline Carbonates as Sintering Aid for Ce0.9Gd0.1O1.95. Budapest, Hungary.
Conference
 15th Conference & Exhibition of the European Ceramic Society
2016/07/25 - 2016/07/27 Poster presentation. Nascimento. NiO-GDC composites obtained by one-step synthesis. Aveiro, Portugal.
Conference
 7th International Conference on Advanced Nanomaterials-ANM
2014/09/28 - 2014/10/02 Poster presentation. Synthesis, sintering and microstructure of NiO/Ni-YSZ anode materials. João Pessoa, Brazil.
Conference
 XIII Brazilian Materials Research Society Meeting
2014/03/31 - 2014/04/04 Course on Rietveld refinement of structures
Other
 Course on Rietveld refinement of structures
Universidade Federal do Ceará, Brazil
2013/06/03 - 2013/06/06 Poster presentation. Preparação de meia-células LSCF/YSZ-Co3O4 por brush painting. Natal, Brazil.
Conference
 57º Congresso Brasileiro de Cerâmica
2012/05/15 - 2012/05/18 Poster presentation. Efeito da adição do Co3O4 na densificação da zircônia estabilizada com 8% mol de ítria. Curitiba, Brazil.
Conference
 56º Congresso Brasileiro de Cerâmica
2011/05/29 - 2011/06/01 Poster presentation. Efeito do teor de Co3O4 na sinterização e microestrutura de cerâmicas de zircônia 4% mol de ítria. Porto de Galinhas, Brazil.
Congress
 55º Congresso Brasileiro de Cerâmica

Jury of academic degree

Topic
Role 		Candidate name (Type of degree)
Institution / Organization
2021/12/29 CARÁTER MULTIFUNCIONAL DE ELETRODOS À BASE DE COBALTITA DE CÁLCIO (Ca3Co2O6)
Thesis Member
 KLIVIA PRICILLIA DE VASCONCELOS MELO (Master)
2021/07/25 PROPRIEDADES MINERALÓGICAS E DIELÉTRICAS DE CERÂMICAS DE ESTEATITA PRODUZIDAS A PARTIR DE TALCO E RESÍDUO DE CAULIM.
(Thesis) Arguer
 Eliandra Dantas de Araújo (Master)
Universidade Federal da Paraíba, Brazil
2021/01/18 INFLUÊNCIA DE VARIÁVEIS DE COMPOSIÇÃO E PROCESSAMENTO NAS PROPRIEDADES DE CORPOS CERÂMICOS OBTIDOS A PARTIR DO RESÍDUO DO POLIMENTO DO PORCELANATO. 2021.
(Thesis) Main arguer
 RAQUEL RODRIGUES DO NASCIMENTO MENEZES (Master)
Universidade Federal da Paraíba, Brazil
2020/01/09 AJUSTE DA CONDUTIVIDADE ELÉTRICA DE UM SEMICONDUTOR ORGÂNICO DO TIPO N ATRAVÉS DE DOPAGEM EM SOLUÇÃO PARA APLICAÇÕES TERMOELÉTRICAS
(Thesis) Main arguer
 ANGEL ROBERTA OLIVEIRA DE SOUSA (Master)
Universidade Federal do Rio Grande do Norte, Brazil

Consulting

Activity description Institution / Organization
2024/02/09 - Current Consulting as honorary professor to lecture materials processing at Yizheng Xiangsheng Composites Co., Ltd.

Course / Discipline taught

Academic session Degree Subject (Type) Institution / Organization
2023/09/18 - 2024/01/24 Class assistant lecture of Electrical, Optical and Magnetic properties Laboratory Engenharia de Materiais (Licenciatura) Universidade de Aveiro, Portugal
2022/09/19 - 2023/01/16 Class assistant lecture of Electrical, Optical and Magnetic properties Laboratory Engenharia de Materiais (Licenciatura) Universidade de Aveiro, Portugal
2014/01/04 - 2014/07/06 Class assistant lecturer Thermodynamics of materials Engenharia de materiais (Bachelor) Universidade Federal do Rio Grande do Norte, Brazil

Journal scientific committee

Journal title (ISSN) Publisher
2019/09/01 - 2019/09/30 Journal of Materials Research and Technology

Mentoring / Tutoring

Topic Student name
2023/11/23 - Current Tuning Grain Boundary Properties through the Sintering of Nano Ce0.9Gd0.1O1.95 Powders with Alkali Salts Henrique Jardim Tidei
2023/05/10 - Current Ceria-based cellular ceramic composites for multi-type energy systems Miguel Angel Illesca Lopez
2023/09/11 - 2024/02/09 Investigating the Incorporation of Recycled Glass in Alumina-Based Composites for Low-Temperature Co-Fired Ceramics (LTCC) Technology Gabija Navašinskaite